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<t>(a)</t> <t>UV–vis</t> <t>diffuse-reflectance</t> spectra of Al 2 O 3 , RuP (66 μmol g –1 )/Al 2 O 3 , and RuCP (66 μmol g –1 )/Al 2 O 3 , FT-IR spectra of (b) RuP (66 μmol g –1 )/Al 2 O 3 , and (c) RuCP (66 μmol g –1 )/Al 2 O 3 before and after irradiation (1.1 mW cm –2 ) at 400 nm for 1 h under a CO 2 atmosphere. The FT-IR spectra of the samples were recorded immediately after the suspended solids were collected by filtration and washed with diethyl ether several times. The measurements were completed within approximately 3 min after filtration.
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(a) UV–vis diffuse-reflectance spectra of Al 2 O 3 , RuP (66 μmol g –1 )/Al 2 O 3 , and RuCP (66 μmol g –1 )/Al 2 O 3 , FT-IR spectra of (b) RuP (66 μmol g –1 )/Al 2 O 3 , and (c) RuCP (66 μmol g –1 )/Al 2 O 3 before and after irradiation (1.1 mW cm –2 ) at 400 nm for 1 h under a CO 2 atmosphere. The FT-IR spectra of the samples were recorded immediately after the suspended solids were collected by filtration and washed with diethyl ether several times. The measurements were completed within approximately 3 min after filtration.

Journal: Journal of the American Chemical Society

Article Title: Elucidating the Origin of Hidden Limitations in Ru-Complex/Ag/Polymeric Carbon Nitride Hybrid Photocatalysts for Visible-Light CO 2 Reduction

doi: 10.1021/jacs.5c21374

Figure Lengend Snippet: (a) UV–vis diffuse-reflectance spectra of Al 2 O 3 , RuP (66 μmol g –1 )/Al 2 O 3 , and RuCP (66 μmol g –1 )/Al 2 O 3 , FT-IR spectra of (b) RuP (66 μmol g –1 )/Al 2 O 3 , and (c) RuCP (66 μmol g –1 )/Al 2 O 3 before and after irradiation (1.1 mW cm –2 ) at 400 nm for 1 h under a CO 2 atmosphere. The FT-IR spectra of the samples were recorded immediately after the suspended solids were collected by filtration and washed with diethyl ether several times. The measurements were completed within approximately 3 min after filtration.

Article Snippet: The prepared materials were characterized by nuclear magnetic resonance (NMR) (JEOL ECA400II) ( 1 H; 400 MHz and 31 P; 168 MHz), X-ray diffraction (XRD) (MiniFlex600, Rigaku; Cu–Kα radiation), UV–vis diffuse-reflectance spectroscopy (DRS) (V-565, Jasco), and Fourier transform infrared (FT-IR) spectroscopy (FT-IR-610, Jasco).

Techniques: Irradiation, Filtration